Study Experimental The Effect of CaCO3 and Fe2O3 Mass Composition Ratio on Calcium Ferrite Phase Formation Base on Local Materials Iron Sand and Limestone

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Published: Jun 1, 2020
DOI: https://doi.org/10.24853/sintek.14.1.27-31

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Mastuki Mastuki
17 Agustus 1945 University Surabaya
AW Brata
17 Agustus 1945 University Surabaya
AG Istiawan
17 Agustus 1945 University Surabaya
B Aditya
17 Agustus 1945 University Surabaya
H Masrufi
17 Agustus 1945 University Surabaya

Abstract

Iron sand contains Fe3O4 which can be produced Fe2O3 and limestone contains dominant CaCO3. Both of these materials are very abundant in Indonesia. Iron sand is generally used as building construction materials, as well as the use of limestone, there has been no development in the management of the combination of the two materials. Because of the abundance of iron sand and limestone which have not yet been developed to the fullest, a study was carried out to manage and develop the product as a follow up to the previous Calcium Ferrite research. This research focuses on analyzing the phase of Calcium Ferrite formed using XRD and SEM-EDX tests. Tests were carried out on samples with a mass ratio of a mixture of Fe2O3 and CaCO3 of 1: 4, 1: 6, 1: 8, and 1:12. The XRD test results showed that the phases formed were dominated by the Ca2Fe2O5 and Ca2Fe9O13 phases. And from the SEM-EDX test results, the results indicate the formation of nano-scale Calcium Ferrite with the composition of elements Ca, Fe, O, and Si.

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[1]
M. Mastuki, A. Brata, A. Istiawan, B. Aditya, and H. Masrufi, “Study Experimental The Effect of CaCO3 and Fe2O3 Mass Composition Ratio on Calcium Ferrite Phase Formation Base on Local Materials Iron Sand and Limestone”, sintek. jurnal. ilm. teknik. mesin, vol. 14, no. 1, pp. 27–31, Jun. 2020.
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Vol. 14 No. 1 (2020): SINTEK JURNAL
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References

H. Putra, I. Satyarno, A. B. Wijatna., Penggunaan Pasir Besi Dari Kulon Progo Dengan Berat Jenis 4, 311 Untuk Mortar Perisai, Forum Teknik Sipil, 2018; 18: 909–920.

Mastuki, M. A. Baqiya, and Darminto., Explorative Synthesis of Magnetic Ca-Fe-O Compounds by Mixing Precipitated CaCO3 from Limestone and Iron Sand Extracted – Fe2O3.H2O, Mater. Sci. Forum, 2015; 827: 203–207.

R. Hayati, A. Budiman, and D. Puryanti., Karakterisasi Suseptibilitas Magnet Barium Ferit Yang Disintesis Dari Pasir Besi Dan Barium Karbonat Menggunakan Metode Metalurgi Serbuk, J. Fis. UNAND, 2016; 5; 187–192.

H. I. Hsiang and R. Q. Yao., Hexagonal Ferrite Powder Synthesis Using Chemical Coprecipitation, Mater. Chem. Phys., 2007; 104: 1–4.

Darminto, M. N. Cholishoh, F. A. Perdana, M. A. Baqiya, M. Y. Cahyono, and Triwikantoro., Preparing Fe3O4 nanoparticles from Fe2+ ions source by co-precipitation process in various pH, AIP Conf. Proc., 2011; 1415: 234–237.

M. Aziz., Batu Kapur Dan Peningkatan Nilai Tambah Serta Spesifikasi Untuk Industri, J. Teknol. Miner. dan Batubara, 2010; 3: 116–131.

E. Asenath-Smith, I. N. Lokuhewa, S. T. Misture, and D. D. Edwards., p-Type thermoelectric properties of the oxygen-deficient perovskite Ca2Fe2O5 in the brownmillerite structure, Journal of Solid State Chemistry, 2010; 183: 1670–1677.

S. P. Mastuki., Analisa Termal Kalsium Ferit Berbasis Bahan Alam Fe2O3•H2O Ekstraksi Pasir Besi, Mek. J. Tek. Mesin, 2018; 4: 7–11.