Effect of Mass Composition on Nano Zircon Synthesize from Local Zircon Sand Using Soda-Precipitation-Calcination-Caustic Fusion Method

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Published: Jul 31, 2024
DOI: https://doi.org/10.24853/jurtek.16.2.169-178
Keywords:
Calcination fusi caustic soda nano zircon NaOH precipitation zircon sand

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Alvika Meta Sari
(Scopus Author ID: 36992719500) Universitas Muhammadiyah Jakarta
Anwar Ilmar Ramadhan
Department of Mechanical Engineering, Faculty of Engineering Universitas Muhammadiyah Jakarta
Istianto Budhi Rahardja
Department of Mechanical Engineering Study Program, Faculty of Engineering and Energy Business, Institut Teknologi PLN
Efrizon Umar
National Research and Innovation Agency
Sri Anastasia Yudistirani
Department of Chemical Engineering, Faculty of Engineering Universitas Muhammadiyah Jakarta
Akmal Imam Faisal
Department of Chemical Engineering, Faculty of Engineering Universitas Muhammadiyah Jakarta
Fikriyansyah Fikriyansyah
Department of Chemical Engineering, Faculty of Engineering Universitas Muhammadiyah Jakarta
Wan Hamzah Azmi
Universiti Malaysia Pahang Al-Sultan Abdullah

Abstract

Zircon sand has the major component of ZrO2 with impurities SiO2, Fe2O2, and TiO2. Zircon sand can be synthesized using various methods, such as caustic fusion method. This research purposed to determine the effect of the mass composition of NaOH on fusion process of zircon sand and to find the optimal mass ration of NaOH on yield and characteristics of nano zircon produced. This research was conducted using caustic fusion and precipitation process to obtain the mass ration of NaOH in best zircon sand fusion (melting) process. The nano zircon obtained was analyzed its size using SEM and chemical composition using FTIR. The result show that the correlation between NaOH ration and yield following the equation y = 0.42x2-2.532x+3.908 and R2 =0.9696. It showed that the higher NaOH composition will reduce the size of nano zircon. The optimum NaOH ratio is 1 : 3.6 with size od 41.983 nm and yield 1.84% which in white, odorless and powder texture. The FTIR spectrum showed the presence of the -Zr-O2 functional groups at wave numbers 600 – 700 cm-1.

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How to Cite
Sari, A. M., Ramadhan, A. I., Rahardja, I. B., Umar, E., Yudistirani, S. A., Faisal, A. I., Fikriyansyah, F., & Azmi, W. H. (2024). Effect of Mass Composition on Nano Zircon Synthesize from Local Zircon Sand Using Soda-Precipitation-Calcination-Caustic Fusion Method. Jurnal Teknologi, 16(2), 169–178. https://doi.org/10.24853/jurtek.16.2.169-178
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Vol. 16 No. 2 (2024): Jurnal Teknologi
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Author Biographies

Alvika Meta Sari, (Scopus Author ID: 36992719500) Universitas Muhammadiyah Jakarta

Department of Chemical Engineering, Faculty of Engineering Universitas Muhammadiyah Jakarta(Profile in Scopus)(Profile in Google Scholar)

Anwar Ilmar Ramadhan, Department of Mechanical Engineering, Faculty of Engineering Universitas Muhammadiyah Jakarta

https://scholar.google.com/citations?user=Y5nDI6UAAAAJ&hl=en Scopus ID: 57193457659

Istianto Budhi Rahardja, Department of Mechanical Engineering Study Program, Faculty of Engineering and Energy Business, Institut Teknologi PLN

https://scholar.google.co.id/citations?user=NNJxE5QAAAAJ&hl=idScopus Author ID: 57211312106

Efrizon Umar, National Research and Innovation Agency

https://scholar.google.co.id/citations?user=7g4cDSYAAAAJ&hl=enScopus Author ID: 54797368100

Sri Anastasia Yudistirani, Department of Chemical Engineering, Faculty of Engineering Universitas Muhammadiyah Jakarta

https://scholar.google.co.id/citations?user=UKWeZL4AAAAJ&hl=en 

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